1-(3,4-DICHLOROPHENYL)TETRAHYDRO-2H-IMIDAZOL-2-ONE

Base Information

• Chemical Name: 1-(3,4-DICHLOROPHENYL)TETRAHYDRO-2H-IMIDAZOL-2-ONE
• CAS No.: 52420-29-8
• Molecular Formula: C₉H₈Cl₂N₂O
• Molecular Weight: 231.081
• Hs Code.: 2933290090
• Mol file: 52420-29-8.mol

Synonyms:AKOS 90512;1-(3,4-Dichlorophenyl)tetrahydro-2H-imidazol-2-one;

Chemical Property of 1-(3,4-DICHLOROPHENYL)TETRAHYDRO-2H-IMIDAZOL-2-ONE

Chemical Property:

• Melting Point: 185-187 °C
• Refractive Index: 1.603
• PSA: 32.34000
• Density: 1.44 g/cm³
• LogP: 2.91680

Purity/Quality:

97% ^*data from raw suppliers

1-(3,4-Dichlorophenyl)imidazolidin-2-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3,4-DICHLOROPHENYL)TETRAHYDRO-2H-IMIDAZOL-2-ONE

There total 2 articles about 1-(3,4-DICHLOROPHENYL)TETRAHYDRO-2H-IMIDAZOL-2-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-Chloro-ethyl)-3-(3,4-dichloro-phenyl)-urea (15145-37-6) → 1-(3,4-dichloro-phenyl)-imidazolidin-2-one (52420-29-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmcl.2009.09.037

Reference yield:

→ 1-(3,4-dichloro-phenyl)-imidazolidin-2-one (52420-29-8)

Guidance literature:

N-<2-Brom-aethyl>-N'-<3,4-dichlor-phenyl>-harnstoff, NaOEt, A., Erwaermen;

Reference yield:

1-(3,4-dichloro-phenyl)-imidazolidin-2-one (52420-29-8) + 1-(5-bromopentyloxy)-3-nitrobenzene → C20H21Cl2N3O4 (1198226-54-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1016/j.bmcl.2009.09.037

upstream raw materials:

1-(2-Chloro-ethyl)-3-(3,4-dichloro-phenyl)-urea

Downstream raw materials:

C₂₀H₂₁Cl₂N₃O₄

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