(E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

Base Information

Chemical Name:(E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide
CAS No.:1033780-02-7
Molecular Formula:C₂₅H₂₆ClN₅O₅S
Molecular Weight:544.031
Hs Code.:

Synonyms:(E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

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Chemical Property of (E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

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Technology Process of (E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

There total 11 articles about (E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033780-25-4
C₂₅H₂₄Cl₂N₄O₅S

: 1033780-02-7
(E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

Guidance literature:: With ammonia; In dichloromethane; water; for 2h;

Reference yield:

: 957513-33-6
4-(3-nitro-pyrazol-1-ylmethyl)-benzoic acid methyl ester

: 1033780-02-7
(E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine / nickel / methanol; water; ethyl acetate / 0.5 h

2: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 2 h / 0 °C

3: lithium hydroxide; water / tetrahydrofuran; methanol / 61.5 h / 0 °C

4: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h

5: ammonia / dichloromethane; water / 2 h

With lithium hydroxide; oxalyl dichloride; ammonia; water; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; HATU; hydrazine; nickel; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate;

Reference yield:

: 54224-24-7
2-(cyclopentyloxy)-1H-isoindole-1,3(2H)-dione

: 1033780-02-7
(E)-4-{3-[2-(3-chloro-4-methanesulfonyl-phenyl)-2-cyclopentyloxyimino-acetylamino]-pyrazol-1-ylmethyl}-benzamide

Guidance literature:: Multi-step reaction with 7 steps

1: hydrazine / methanol; dichloromethane / 4 h / 25 °C

2: methanol / 2 h / 70 °C

3: lithium hydroxide; water / methanol / 1 h / 0 °C

4: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 2 h / 0 °C

5: lithium hydroxide; water / tetrahydrofuran; methanol / 61.5 h / 0 °C

6: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h

7: ammonia / dichloromethane; water / 2 h

With lithium hydroxide; oxalyl dichloride; ammonia; water; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; HATU; hydrazine; In tetrahydrofuran; methanol; dichloromethane; water;