1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

Base Information

Chemical Name:1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol
CAS No.:96579-20-3
Molecular Formula:C₂₄H₄₂O₁₂S₄
Molecular Weight:650.854
Hs Code.:

Synonyms:1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

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Chemical Property of 1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

Chemical Property:

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Technology Process of 1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

There total 4 articles about 1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 488-23-3
1,2,3,4-Tetramethylbenzene

: 96579-20-3
1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

Guidance literature:: Multi-step reaction with 4 steps

1: aq. HCl / decane

2: (i) Na, EtOH, (ii) /BRN= 2445231/, toluene

3: LiAlH₄ / tetrahydrofuran

4: collidine / CHCl₃

With 2,3,5-trimethyl-pyridine; hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; decane; chloroform;
DOI:10.1021/ja01059a024

Reference yield:

: 29002-55-9
1,2-bis(chloromethyl)-3,4,5,6-tetramethylbenzene

: 96579-20-3
1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Na, EtOH, (ii) /BRN= 2445231/, toluene

2: LiAlH₄ / tetrahydrofuran

3: collidine / CHCl₃

With 2,3,5-trimethyl-pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; chloroform;
DOI:10.1021/ja01059a024

Reference yield:

: 96270-48-3
1.2.3.4-Tetramethyl-5.6-bis-<2.2-diaethoxycarbonyl-propyl>-benzol

: 96579-20-3
1,2,3,4-Tetramethyl-5,6-bis-<(2,2-bis-methansulfonyloxymethyl)-propyl>-benzol

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran

2: collidine / CHCl₃

With 2,3,5-trimethyl-pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; chloroform;
DOI:10.1021/ja01059a024