N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

Base Information

Chemical Name:N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide
CAS No.:412009-89-3
Molecular Formula:C₂₂H₂₆F₃NO₇
Molecular Weight:473.446
Hs Code.:

Synonyms:N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

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Chemical Property of N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

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Technology Process of N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

There total 7 articles about N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 412009-96-2
N-(3,5-di(methoxymethyoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethylamine

: 407-25-0
trifluoroacetic anhydride

: 412009-89-3
N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

Guidance literature:: With pyridine; at 0 ℃; for 0.333333h;
DOI:10.1248/cpb.54.1662

Reference yield:

: 26267-67-4
3,5-di(methoxymethyloxy)-4-methoxybenzyl alcohol

: 412009-89-3
N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / palladium acetate; pyridine; O₂ / toluene / 2.5 h / 90 °C

2: methanol / 0.33 h / 20 °C

3: 3.80 g / NaBH₄ / methanol / 0.83 h / 20 °C

4: 85 percent / pyridine / 0.33 h / 0 °C

With pyridine; sodium tetrahydroborate; oxygen; palladium diacetate; In methanol; toluene;
DOI:10.1248/cpb.54.1662

Reference yield:

: 4-(2-{[1-(4-Methoxy-3,5-bis-methoxymethoxy-phenyl)-meth-(E)-ylidene]-amino}-ethyl)-phenol

: 412009-89-3
N-(3,5-di(methoxymethoxy)-4-methoxy)benzyl-N-(4-hydroxyphenyl)ethyltrifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 3.80 g / NaBH₄ / methanol / 0.83 h / 20 °C

2: 85 percent / pyridine / 0.33 h / 0 °C

With pyridine; sodium tetrahydroborate; In methanol;
DOI:10.1248/cpb.54.1662