2-methyl 4-phenylthio thiochromane

Base Information

Chemical Name:2-methyl 4-phenylthio thiochromane
CAS No.:111191-83-4
Molecular Formula:C₁₆H₁₆S₂
Molecular Weight:272.435
Hs Code.:

Synonyms:2-methyl 4-phenylthio thiochromane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl 4-phenylthio thiochromane

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Technology Process of 2-methyl 4-phenylthio thiochromane

There total 3 articles about 2-methyl 4-phenylthio thiochromane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 108-98-5
thiophenol

: 111191-83-4
2-methyl 4-phenylthio thiochromane

Guidance literature:: phosphotungstic acid; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2005.08.156

Reference yield: 48.0%

: 108-98-5
thiophenol

: 123-73-9,4170-30-3
crotonaldehyde

: 60466-63-9
1,1,3-(trisphenylthio)butane

: 111191-83-4
2-methyl 4-phenylthio thiochromane

Guidance literature:: With KSF Montmorillonite; In toluene; Heating;

Reference yield: 39.0%

: 372-48-5
2-fluoropyridine

: 51207-25-1,67529-33-3,104113-36-2,4170-80-3
ethylphenylsulfoxide

: 111191-83-4
2-methyl 4-phenylthio thiochromane

Guidance literature:: With trifluoromethylsulfonic anhydride; In dichloromethane; at -43 - 20 ℃; for 10h; Schlenk technique;
DOI:10.1039/c8ob00860d