dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester
• CAS No.: 588706-87-0
• Molecular Formula: C₂₃H₂₈N₂O₇S₂
• Molecular Weight: 508.617

Synonyms:dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester

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Technology Process of dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester

There total 4 articles about dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

potassium ethyl xanthogenate (140-89-6) + acetic acid 5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl ester → dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester (588706-87-0)

Guidance literature:

In acetic acid; acetonitrile; at 0 - 20 ℃;

DOI:10.1021/ol035027c

Reference yield:

2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane (21473-46-1) → dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester (588706-87-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 23 percent / sodium methoxide / methanol / 2.33 h / -55 - -10 °C

2: Et₃N / 1 h / 20 °C

3: DMAP / 2 h / 20 °C

4: 69 percent / acetonitrile; acetic acid / 0 - 20 °C

With dmap; sodium methylate; triethylamine; In methanol; acetic acid; acetonitrile; 2: Henry reaction;

DOI:10.1021/ol035027c

Reference yield:

5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-pentanal (588706-85-8) → dithiocarbonic acid S-[5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-1-nitromethyl-pentyl] ester O-ethyl ester (588706-87-0)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / 1 h / 20 °C

2: DMAP / 2 h / 20 °C

3: 69 percent / acetonitrile; acetic acid / 0 - 20 °C

With dmap; triethylamine; In acetic acid; acetonitrile; 1: Henry reaction;

DOI:10.1021/ol035027c

upstream raw materials:

potassium ethyl xanthogenate

2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane

5-(4-benzyloxy-3-methoxy-phenyl)-4-nitro-pentanal

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