C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

Base Information

Chemical Name:C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾
CAS No.:1335283-34-5
Molecular Formula:C₂F₃O₂*C₄₉H₆₃N₂O₁₀
Molecular Weight:953.063
Hs Code.:

C<sub>2</sub>F<sub>3</sub>O<sub>2</sub><sup>(1-)</sup>*C<sub>49</sub>H<sub>63</sub>N<sub>2</sub>O<sub>10</sub><sup>(1+)</sup>

Synonyms:C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

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Chemical Property of C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

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Technology Process of C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

There total 12 articles about C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₅₇H₇₁N₂O₁₁⁽¹⁺⁾*Cl^(1-)

: 76-05-1
trifluoroacetic acid

: 1335283-34-5
C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

Guidance literature:: With methoxybenzene; at 23 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ja206339s

Reference yield:

: 31558-41-5
4-bromo-2,5-dimethoxybenzaldehyde

: 1335283-34-5
C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1: dihydrogen peroxide; potassium hydroxide / methanol; water / 1.5 h / 65 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium hydroxide; tert-butyl XPhos / 1,4-dioxane; water / 15 h / 80 °C / Inert atmosphere

3: sodium hydrogencarbonate / N,N-dimethyl-formamide / 30 h / 23 - 50 °C / Inert atmosphere

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 18 h / 0 - 23 °C / Inert atmosphere

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 30 h / 23 °C / Inert atmosphere

6: methoxybenzene / 0.33 h / 23 °C / Inert atmosphere

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; di-isopropyl azodicarboxylate; dihydrogen peroxide; sodium hydrogencarbonate; methoxybenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; potassium hydroxide; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja206339s

Reference yield:

: 1127303-67-6
1,3,3-trimethyl-2-((1E,3E)-4-(N-phenylacetamido)buta-1,3-dien-1-yl)-3H-indolium chloride

: 1335283-34-5
C₂F₃O₂^(1-)*C₄₉H₆₃N₂O₁₀⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 1.5 h / 23 - 50 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 30 h / 23 °C / Inert atmosphere

3: methoxybenzene / 0.33 h / 23 °C / Inert atmosphere

With pyridine; dmap; methoxybenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/ja206339s