C₃₅H₄₆O₂Si

Base Information

Chemical Name:C₃₅H₄₆O₂Si
CAS No.:1429123-42-1
Molecular Formula:C₃₅H₄₆O₂Si
Molecular Weight:526.835
Hs Code.:

C<sub>35</sub>H<sub>46</sub>O<sub>2</sub>Si

Synonyms:C₃₅H₄₆O₂Si

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Chemical Property of C₃₅H₄₆O₂Si

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Technology Process of C₃₅H₄₆O₂Si

There total 12 articles about C₃₅H₄₆O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1429123-41-0
C₃₅H₄₈O₂Si

: 1429123-42-1
C₃₅H₄₆O₂Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; tert-butyl alcohol; In dichloromethane; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ol400508s

Reference yield:

: 861909-36-6
(2E,4Z)-5-iodo-2,4-dimethylpenta-2,4-dienal

: 1429123-42-1
C₃₅H₄₆O₂Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / -78 °C / Inert atmosphere

2.1: trimethylaluminum / toluene; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 1 h / -20 - 0 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5.1: lithium tert-butoxide / hexane; dichloromethane / 20 °C / Inert atmosphere

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate / benzene / 18 h / 65 - 125 °C / Darkness; Inert atmosphere; Schlenk technique

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 55 °C / Molecular sieve; Inert atmosphere

8.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

9.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

10.1: sodium hydrogencarbonate; tert-butyl alcohol; Dess-Martin periodane / dichloromethane / 0.08 h / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; trimethylaluminum; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium tert-butoxide; tert-butyl alcohol; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 6.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol400508s

Reference yield:

: 1429123-31-8
C₂₀H₂₄INO₄

: 1429123-42-1
C₃₅H₄₆O₂Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: trimethylaluminum / toluene; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 1 h / -20 - 0 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.1: lithium tert-butoxide / hexane; dichloromethane / 20 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate / benzene / 18 h / 65 - 125 °C / Darkness; Inert atmosphere; Schlenk technique

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 55 °C / Molecular sieve; Inert atmosphere

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

8.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

9.1: sodium hydrogencarbonate; tert-butyl alcohol; Dess-Martin periodane / dichloromethane / 0.08 h / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; tetrabutyl ammonium fluoride; trimethylaluminum; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; lithium tert-butoxide; tert-butyl alcohol; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 5.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol400508s