ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate

Base Information

Chemical Name:ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate
CAS No.:1187785-00-7
Molecular Formula:C₂₇H₄₂O₆Si
Molecular Weight:490.712
Hs Code.:

Synonyms:ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate

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Chemical Property of ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate

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Technology Process of ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate

There total 1 articles about ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187785-12-1
C₂₃H₃₆O₅Si

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 1187785-00-7
ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate

Guidance literature:: In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2009.06.059

Reference yield: 75.0%

: 1187785-00-7
ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate

: 1187785-13-2
C₂₅H₄₀O₅Si

Guidance literature:: ethyl (4S,2E,7E)-9-acetoxy-10-(benzyloxy)-4-(tert-butyldimethylsilyloxy)deca-2,7-dienoate; With potassium carbonate; In ethanol; at 0 - 20 ℃; for 6h; Inert atmosphere;

With ammonium chloride; In ethanol; water;
DOI:10.1016/j.tet.2009.06.059