(2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester

Base Information

Chemical Name:(2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester
CAS No.:1038925-80-2
Molecular Formula:C₂₂H₃₆N₂O₇Si
Molecular Weight:468.623
Hs Code.:

Synonyms:(2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester

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Chemical Property of (2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester

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Technology Process of (2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester

There total 1 articles about (2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 39994-75-7
L-threonine methyl ester hydrochloride

: 104499-27-6,146346-84-1
(S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid

: 1038925-80-2
(2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester

Guidance literature:: (S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid; With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

L-threonine methyl ester hydrochloride; With 4-methyl-morpholine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/b802477d

Reference yield:

: 1038925-80-2
(2S,3R)-2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionylamino]-3-hydroxybutyric acid methyl ester

: 1095980-78-1
C₂₂H₃₄N₂O₆Si

Guidance literature:: With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1039/b802477d