methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

Base Information

Chemical Name:methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside
CAS No.:1598426-42-6
Molecular Formula:C₃₇H₄₀O₈Si
Molecular Weight:640.805
Hs Code.:

Synonyms:methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

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Technology Process of methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

There total 8 articles about methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 613-90-1
benzoyl cyanide

: 401593-03-1
methyl 2-O-benzoyl-6-O-[(tert-butyl)diphenylsilyl]-α-D-galactopyranoside

: 1598426-42-6
methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; at -78 ℃; for 2h; Molecular sieve; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01446

Reference yield: 76.0%

: 613-90-1
benzoyl cyanide

: 114217-35-5
methyl 6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranoside

: 1598426-42-6
methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; chloroform; at -78 ℃; for 10h; regioselective reaction; Schlenk technique; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.orglett.8b01446

Reference yield: 76.0%

: 613-90-1
benzoyl cyanide

: 114217-35-5
methyl 6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranoside

: 1598426-42-6
methyl 6-O-tert-butyldiphenylsilyl-2,4-di-O-benzoyl-α-D-galactopyranoside

: methyl 3-O-benzoyl-6-O-[(tert-butyl)diphenylsilyl]-α-D-galactopyranoside

: methyl 2,3-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; chloroform; at -78 ℃; for 10h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01446