7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

Base Information

Chemical Name:7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine
CAS No.:1610435-69-2
Molecular Formula:C₅₀H₄₄N₂O₄S₃
Molecular Weight:833.108
Hs Code.:

Synonyms:7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

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Chemical Property of 7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

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Technology Process of 7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

There total 7 articles about 7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1610435-66-9
9-butyl-N,N-diphenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazol-2-amine

: 1610435-68-1
5-(3,4-bis(methoxymethoxy)phenyl)-5''-bromo-2,2'-5',2''-terthiophene

: 1610435-69-2
7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c4ta01286k

Reference yield:

: 1443920-03-3
7-bromo-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

: 1610435-69-2
7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 15 h / 80 °C

2: sodium carbonate; water; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; potassium acetate; sodium carbonate; In N,N-dimethyl-formamide; 1: |Miyaura Borylation Reaction / 2: |Suzuki Coupling;
DOI:10.1039/c4ta01286k

Reference yield:

: 1610435-67-0
5-(3,4-bis(methoxymethoxy)phenyl)-2,2'-5',2''-terthiophene

: 1610435-69-2
7-(5''-(3,4-bis(methoxymethoxy)phenyl)-[2,2':5',2''-terthiophen]-5-yl)-9-butyl-N,N-diphenyl-9H-carbazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / chloroform / 2 h / 0 °C

2: sodium carbonate; water; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium carbonate; In chloroform; N,N-dimethyl-formamide; 2: |Suzuki Coupling;
DOI:10.1039/c4ta01286k