Technology Process of C41H46N2O8S
There total 6 articles about C41H46N2O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 72h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 18 h / Heating / reflux
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C
4: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C
With
oxalyl dichloride; tetrabutyl ammonium fluoride; potassium carbonate; caesium carbonate; dimethyl sulfoxide; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / tetrahydrofuran / 0.25 h / 20 °C
2: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 18 h / Heating / reflux
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
4: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C
5: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C
With
oxalyl dichloride; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; caesium carbonate; dimethyl sulfoxide; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;