methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

Base Information

Chemical Name:methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate
CAS No.:1431505-02-0
Molecular Formula:C₁₇H₁₆F₃NO₅S
Molecular Weight:403.379
Hs Code.:

Synonyms:methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

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Chemical Property of methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

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Technology Process of methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

There total 7 articles about methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431504-99-2
methyl 3-amino-5-(methylsulfonyl)-4-phenoxybenzoate

: 76-05-1
trifluoroacetic acid

: 1431505-02-0
methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

Guidance literature:: With sodium tetrahydroborate; at 70 ℃;

Reference yield:

: 2494-79-3
4-chloro-3-(chlorosulfonyl)benzoic acid

: 1431505-02-0
methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

Guidance literature:: Multi-step reaction with 7 steps

1: sodium sulfite / water / 3 h / 0 - 20 °C

2: sodium hydroxide / water; methanol / 72 h / 20 °C

3: sulfuric acid; nitric acid / 1 h / 0 - 110 °C

4: sodium hydrogencarbonate / water / 85 °C

5: thionyl chloride / 60 °C

6: ammonium chloride; iron / water; ethanol / 2.25 h / 85 °C

7: sodium tetrahydroborate / 70 °C

With sodium tetrahydroborate; thionyl chloride; sulfuric acid; nitric acid; iron; sodium hydrogencarbonate; ammonium chloride; sodium hydroxide; sodium sulfite; In methanol; ethanol; water;

Reference yield:

: 32548-10-0
3-methylsulfonyl-4-chloro-5-nitrobenzoic acid

: 1431505-02-0
methyl 3-(methylsulfonyl)-4-phenoxy-5-(2,2,2-trifluoroethylamino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / water / 85 °C

2: thionyl chloride / 60 °C

3: ammonium chloride; iron / water; ethanol / 2.25 h / 85 °C

4: sodium tetrahydroborate / 70 °C

With sodium tetrahydroborate; thionyl chloride; iron; sodium hydrogencarbonate; ammonium chloride; In ethanol; water;