5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propen-1-yl)-,(5aS,6S,12S,14aS)-

Base Information

• Chemical Name: 5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propen-1-yl)-,(5aS,6S,12S,14aS)-
• CAS No.: 111468-06-5
• Molecular Formula: C₂₂H₂₅N₃O₅
• Molecular Weight: 411.458

Synonyms:5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propenyl)-,(5aS,6S,12S,14aS)- (9CI); 5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propenyl)-,[5aS-(5aa,6b,12a,14ab)]-; (+)-Cyclotryprostatin A;Cyclotryprostatin A; Cyclotryprostatine A

Chemical Property of 5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propen-1-yl)-,(5aS,6S,12S,14aS)-

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Technology Process of 5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propen-1-yl)-,(5aS,6S,12S,14aS)-

There total 1 articles about 5H,14H-Pyrrolo[1'',2'':4',5']pyrazino[1',2':1,6]pyrido[3,4-b]indole-5,14-dione,1,2,3,5a,6,11,12,14a-octahydro-5a,6-dihydroxy-9-methoxy-12-(2-methyl-1-propen-1-yl)-,(5aS,6S,12S,14aS)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

fumitremorgin B (111139-38-9,12626-17-4) → 13-oxoverruculogen (1054470-71-1) + verruculogen (12771-72-1) + 12,13-Dihydroxyfumitremorgin C (111468-05-4,111468-06-5,111427-99-7)

Guidance literature:

With FtmF oxygenase gene; at 30 ℃; for 24h; pH=7; aq. buffer; Enzymatic reaction;

DOI:10.1002/cbic.201000562

Reference yield: 66.0%

12,13-Dihydroxyfumitremorgin C (111468-05-4,111468-06-5,111427-99-7) + 3,3-dimethyl-allyl chloride (503-60-6) → fumitremorgin B (111139-38-9,12626-17-4)

Guidance literature:

With potassium hydroxide; 18-crown-6 ether; In benzene;

DOI:10.1016/S0040-4039(00)85436-2

Reference yield:

12,13-Dihydroxyfumitremorgin C (111468-05-4,111468-06-5,111427-99-7) → fumitremorgin B (111139-38-9,12626-17-4)

Guidance literature:

With FtmH; FtmPT₂; Enzymatic reaction;

DOI:10.1039/b908392h

upstream raw materials:

fumitremorgin B

Downstream raw materials:

fumitremorgin B

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