Technology Process of C21H25NO8
There total 3 articles about C21H25NO8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium fluoride; N,N-dimethylammonium chloride;
In
xylene;
for 48h;
Heating;
DOI:10.1248/cpb.34.1628
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 92.5 percent / silicagel (200-400 mesh ASTM), NaBH4 / propan-2-ol; CHCl3 / 2 h
2: 87 percent / dimethylammonium chloride, KF / xylene / 48 h / Heating
With
potassium fluoride; sodium tetrahydroborate; N,N-dimethylammonium chloride; silica gel;
In
chloroform; isopropyl alcohol; xylene;
DOI:10.1248/cpb.34.1628
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 83 percent / dimethylammonium chloride, KF / toluene / 5 h / Heating
2: 92.5 percent / silicagel (200-400 mesh ASTM), NaBH4 / propan-2-ol; CHCl3 / 2 h
3: 87 percent / dimethylammonium chloride, KF / xylene / 48 h / Heating
With
potassium fluoride; sodium tetrahydroborate; N,N-dimethylammonium chloride; silica gel;
In
chloroform; isopropyl alcohol; toluene; xylene;
DOI:10.1248/cpb.34.1628