(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

Base Information

Chemical Name:(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester
CAS No.:1032191-86-8
Molecular Formula:C₁₅H₁₈F₃NO₂
Molecular Weight:301.309
Hs Code.:

Synonyms:(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

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Technology Process of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

There total 2 articles about (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 69143-05-1
(E)-4-methyl-pent-2-en-1-ol

: 75999-66-5
(Z)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidoyl chloride

: 1032191-86-8
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/anie.200601731

Reference yield: 71.0%

: 69143-05-1
(E)-4-methyl-pent-2-en-1-ol

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 1032191-86-8
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

Guidance literature:: (E)-4-methyl-pent-2-en-1-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

N-(4-methoxyphenyl)trifluoroacetimidoyl chloride; In tetrahydrofuran; mineral oil; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.200900712

Reference yield: 76.0%

: 1032191-86-8
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 4-methyl-pent-2-enyl ester

: 913974-34-2
(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-isopropylallyl)acetamide

Guidance literature:: With di-μ-chlorobis[η⁵-(S)-(S_p)-2-(2'-(4'-methylethyl)oxazolinyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadiene)ferrocene]dipalladium; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; silver nitrate; In dichloromethane; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900712