(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

Base Information

Chemical Name:(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide
CAS No.:499993-27-0
Molecular Formula:C₂₂H₂₇NO₃S
Molecular Weight:385.527
Hs Code.:

Synonyms:(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

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Technology Process of (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

There total 3 articles about (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54256-37-0
2-(ethylthio)acetyl chloride

: Benzyl-[2-(3,4-dimethoxy-phenyl)-prop-(Z)-ylidene]-amine

: 499993-28-1
(Z)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

: 499993-27-0
(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/jo026471g

Reference yield:

: 40181-00-8
2-(3,4-di-methoxyphenyl)propionaldehyde

: 499993-27-0
(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 24 h / Heating

2: pyridine / CH₂Cl₂ / 2 h / 25 °C

With pyridine; In dichloromethane; benzene;
DOI:10.1021/jo026471g

Reference yield:

: 51698-53-4
2‐(3,4‐dimethoxyphenyl)propionitrile

: 499993-27-0
(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)prop-1-enyl]-2-ethylsulfanylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diisobutylalumminum hydride / toluene / 1.5 h / 0 °C

2: benzene / 24 h / Heating

3: pyridine / CH₂Cl₂ / 2 h / 25 °C

With pyridine; diisobutylaluminium hydride; In dichloromethane; toluene; benzene;
DOI:10.1021/jo026471g