Technology Process of C32H32O11S
There total 4 articles about C32H32O11S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 20 ℃;
for 2h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / Cooling with ice
1.2: 1 h
1.3: 1 h / -78 °C
2.1: acetic acid; water / 15 h / 100 °C
3.1: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice
With
pyridine; water; isopropylmagnesium chloride; acetic acid; lithium chloride;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / Cooling with ice
1.2: 1 h
1.3: 1 h / -78 °C
2.1: acetic acid; water / 15 h / 100 °C
3.1: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice
With
pyridine; water; isopropylmagnesium chloride; acetic acid; lithium chloride;
In
tetrahydrofuran; dichloromethane;