C₂₃H₂₀ClN₅O₃S

Base Information

Chemical Name:C₂₃H₂₀ClN₅O₃S
CAS No.:1333394-07-2
Molecular Formula:C₂₃H₂₀ClN₅O₃S
Molecular Weight:481.962
Hs Code.:

C<sub>23</sub>H<sub>20</sub>ClN<sub>5</sub>O<sub>3</sub>S

Synonyms:C₂₃H₂₀ClN₅O₃S

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Chemical Property of C₂₃H₂₀ClN₅O₃S

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Technology Process of C₂₃H₂₀ClN₅O₃S

There total 8 articles about C₂₃H₂₀ClN₅O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1333393-85-3
C₁₅H₁₅N₅O

: 216955-76-9
(E)-2-(3’ chlorophenyl)ethene-1-sulfonyl chloride

: 1333394-07-2
C₂₃H₂₀ClN₅O₃S

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2011.07.023

Reference yield:

: 100-55-0
3-hydroxymethylpyridin

: 1333394-07-2
C₂₃H₂₀ClN₅O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide; tetra-(n-butyl)ammonium iodide; triethylamine; N-tosylimidazole / N,N-dimethyl-formamide / 21 h / 100 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / ethanol; water / 24 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 2.5 h / 20 °C

4: sodium carbonate / tetrahydrofuran; water / 3 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; tetra-(n-butyl)ammonium iodide; sodium carbonate; sodium L-ascorbate; triethylamine; N-tosylimidazole; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.023

Reference yield:

: 864528-33-6
3-(azidomethyl)pyridine

: 1333394-07-2
C₂₃H₂₀ClN₅O₃S

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / ethanol; water / 24 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 2.5 h / 20 °C

3: sodium carbonate / tetrahydrofuran; water / 3 h / 20 °C

With copper(ll) sulfate pentahydrate; sodium carbonate; sodium L-ascorbate; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.07.023