allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

Base Information

Chemical Name:allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside
CAS No.:1616860-60-6
Molecular Formula:C₉₄H₁₀₀Cl₆N₂O₂₅
Molecular Weight:1870.54
Hs Code.:

allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

Synonyms:allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

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Chemical Property of allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

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Technology Process of allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

There total 1 articles about allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1616860-55-9
allyl (methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

: allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-D-glucopyranoside-trichloroacetimidate

: 1616860-60-6
allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

Guidance literature:: allyl (methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside; allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-D-glucopyranoside-trichloroacetimidate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere; Molecular sieve;
DOI:10.1002/adsc.201400269

Reference yield: 78.0%

: 1616860-60-6
allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

: 1616860-61-7
allyl (methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: With pyridine; hydrazine hydrate; acetic acid; allyl alcohol; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1002/adsc.201400269

Reference yield:

: 1616860-60-6
allyl (methyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1→3)-(4,6-di-Obenzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1→4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-Dglucopyranoside

: C₉₄H₁₀₆N₂O₂₅

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In N,N-dimethyl acetamide; benzene; at 80 ℃; Inert atmosphere;
DOI:10.1002/adsc.201400269