HSC₆H₄NHCONHC₆H₅

Base Information

• Chemical Name: HSC₆H₄NHCONHC₆H₅
• CAS No.: 943414-53-7
• Molecular Formula: C₁₃H₁₂N₂OS
• Molecular Weight: 244.317
• Mol file: 943414-53-7.mol

Synonyms:HSC₆H₄NHCONHC₆H₅

Chemical Property of HSC₆H₄NHCONHC₆H₅

Chemical Property:

Purity/Quality:

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Technology Process of HSC₆H₄NHCONHC₆H₅

There total 1 articles about HSC₆H₄NHCONHC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

bis-[4-(N'-phenyl-ureido)-phenyl]-disulfide (52017-43-3) → HSC6H4NHCONHC6H5 (943414-53-7)

Guidance literature:

With hydrogenchloride; triphenylphosphine; In 1,4-dioxane; water; at 60 ℃; Inert atmosphere;

DOI:10.1021/ic9021068

Reference yield: 98.0%

potassium tetrachloroaurate(III) (13682-61-6) + HSC6H4NHCONHC6H5 (943414-53-7) → Au(1+)*SC6H4NHCONHC6H5(1-)=Au(SC6H4NHCONHC6H5) (1210067-70-1)

Guidance literature:

With 2,2'-thiodiethanol; In methanol; H₂O; tetrahydrofuran; under N2; 2,2'-thiodiethanol added dropwise to soln. of KAuCl4 in MeOH-H2O; stirred; ligand in THF added; stirred for 30 min; ppt. sepd.; washed with H2O, MeOH and Et2O; dried under vac.; elem. anal.;

DOI:10.1021/ic9021068

Reference yield:

HSC6H4NHCONHC6H5 (943414-53-7) + [Au2{μ-Ph2PN(C6H4OCH3-p)PPh2}Cl2] (1578268-25-3) → C57H49Au2N5O3P2S2

Guidance literature:

With triethylamine; In dichloromethane; Inert atmosphere;

DOI:10.1002/chem.201500493

upstream raw materials:

bis-[4-(N'-phenyl-ureido)-phenyl]-disulfide

Downstream raw materials:

Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)