[3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

Base Information

Chemical Name:[3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester
CAS No.:146495-76-3
Molecular Formula:C₁₆H₁₇N₅O₃S
Molecular Weight:359.409
Hs Code.:

Synonyms:[3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

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Chemical Property of [3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

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Technology Process of [3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

There total 6 articles about [3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 28241-61-4
ammonia thiocyanic acid

: 146495-71-8
[3-(5-Methyl-2-phenyl-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

: 146495-76-3
[3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

Guidance literature:: With bromine; In acetic acid; at 7 - 8 ℃; for 0.75h;

Reference yield:

: 58663-02-8
5-phenyl-7-methylpyrazolo<4,3-c><1,2,5>oxadiazin-3(5H)-one

: 146495-76-3
[3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / CH₂Cl₂ / 0.75 h

2: 79 percent / 99 percent hydrazine hydrate / 10 percent Pd/C / methanol / 0.08 h / Heating

3: 76 percent / sodium nitrite, 1 N HCl / H₂O; methanol / 2 h

4: 87 percent / ethanol; H₂O / 2 h / Irradiation

5: 50 percent / H₂ / 10 percent Pd/C / methanol; acetic acid / 2 h

6: 78 percent / bromine / acetic acid / 0.75 h / 7 - 8 °C

With hydrogenchloride; hydrogen; bromine; hydrazine hydrate; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; acetic acid;

Reference yield:

: 146495-66-1
(3-Methyl-1-phenyl-1H-pyrazolo[3,4-d]oxazol-5-ylamino)-acetic acid ethyl ester

: 146495-76-3
[3-(5-Methyl-2-phenyl-4-thiocyanato-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / H₂ / 10 percent Pd/C / methanol; acetic acid / 2 h

2: 78 percent / bromine / acetic acid / 0.75 h / 7 - 8 °C

With hydrogen; bromine; palladium on activated charcoal; In methanol; acetic acid;