dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane

Base Information

Chemical Name:dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane
CAS No.:955119-88-7
Molecular Formula:C₃₆H₄₄Si₂
Molecular Weight:532.916
Hs Code.:

Synonyms:dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane

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Chemical Property of dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane

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Technology Process of dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane

There total 1 articles about dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848758-12-3
3,5-dimethyl-4-trimethylsilyl-bromobenzene

: chlorodimethyl(2-methyl-4-phenylcyclopentadienyl)silane

: 769-86-8
2-methylazulene

: 955119-88-7
dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane

Guidance literature:: 3,5-dimethyl-4-trimethylsilyl-bromobenzene; With tert.-butyl lithium; In hexane; di-isopropyl ether; pentane; at -70 - -10 ℃; for 1h;

2-methylazulene; In hexane; di-isopropyl ether; pentane; at 20 ℃; for 1h;

chlorodimethyl(2-methyl-4-phenylcyclopentadienyl)silane; With 1-methyl-1H-imidazole; In tetrahydrofuran; hexane; di-isopropyl ether; pentane; at 0 - 20 ℃; for 1h;

Reference yield:

: 955119-88-7
dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane

: 13499-05-3
hafnium tetrachloride

: 955119-90-1
dichloro{1,1'-dimethylsilylene(2-methyl-4-phenylcyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-4H-azulenyl)}hafnium

Guidance literature:: dimethyl(2-methyl-4-phenyl-2,4-cyclopentadienyl)(2-methyl-4-(4-trimethylsilyl-3,5-dimethylphenyl)-1,4-dihydroazulenyl)silane; With n-butyllithium; In diethyl ether; hexane; at 0 - 20 ℃; for 2h;

hafnium tetrachloride; In diethyl ether; hexane; toluene; at -60 - 20 ℃; for 2h;