Technology Process of C38H49NO6Si2
There total 13 articles about C38H49NO6Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; sodium hydroxide;
In
methanol; dichloromethane;
at 0 ℃;
DOI:10.1021/jo301638z
- Guidance literature:
-
With
dihydrogen peroxide; sodium hydroxide;
In
methanol; dichloromethane; water;
at 0 ℃;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 10 steps
1: thionyl chloride / acetonitrile / 0 - 20 °C
2: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C
3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C
4: diisobutylaluminium hydride / dichloromethane / -78 °C
5: methylmagnesium bromide / diethyl ether / 0 °C
6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C
7: ozone / dichloromethane / -78 °C
8: N-ethyl-N,N-diisopropylamine; titanium tetrachloride; chloro-trimethyl-silane / dichloromethane / 0 °C
9: trifluoroacetyl chloride; pyridine / dichloromethane / 20 °C
10: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane / 0 °C
With
pyridine; 2,6-dimethylpyridine; chloro-trimethyl-silane; thionyl chloride; oxalyl dichloride; methylmagnesium bromide; dihydrogen peroxide; titanium tetrachloride; diisobutylaluminium hydride; ozone; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetyl chloride; sodium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo301638z
