(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

Base Information

Chemical Name:(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure
CAS No.:81149-14-6
Molecular Formula:C₂₃H₂₄N₂O₅
Molecular Weight:408.454
Hs Code.:

(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzo<F>chinolin-2-carbonsaeure

Synonyms:(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

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Chemical Property of (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

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Technology Process of (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

There total 4 articles about (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 81149-15-7
(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

: 81149-14-6
(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

Guidance literature:: With sodium hydroxide; In methanol; water; at 55 ℃; for 2h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 81149-14-6
(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / tetrahydrofuran; pyridine / 20 °C

2: 65 percent / 2 N NaOH / methanol; H₂O / 2 h / 55 °C

With sodium hydroxide; In tetrahydrofuran; pyridine; methanol; water;

Reference yield:

: 65291-20-5
(2R,4aR,10bR)-7-Amino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

: 81149-14-6
(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / tetrahydrofuran; pyridine / 20 °C

2: 65 percent / 2 N NaOH / methanol; H₂O / 2 h / 55 °C

With sodium hydroxide; In tetrahydrofuran; pyridine; methanol; water;