p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside
CAS No.:945219-31-8
Molecular Formula:C₂₁H₃₀NO₁₂P
Molecular Weight:519.442
Hs Code.:

Synonyms:p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

There total 4 articles about p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945219-27-2
C₁₆H₂₄Cl₃N₂O₁₁P

: 150-76-5
4-methoxy-phenol

: 945219-31-8
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

: C₂₁H₃₀NO₁₂P

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -15 - 20 ℃; Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2007.04.150

Reference yield:

: 122119-28-2
C₂₆H₃₀NO₁₂P

: 945219-31-8
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / NH₃ / tetrahydrofuran / 0.67 h / 0 °C

2: 82 percent / DBU / CH₂Cl₂ / 3 h / 20 °C

3: TMSOTf; 4A MS / CH₂Cl₂ / -15 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; ammonia; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2007.04.150

Reference yield:

: C₁₄H₂₄NO₁₁P

: 945219-31-8
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-N-dimethylphosphoryl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / DBU / CH₂Cl₂ / 3 h / 20 °C

2: TMSOTf; 4A MS / CH₂Cl₂ / -15 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/j.tetlet.2007.04.150