2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole

Base Information

• Chemical Name: 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole
• CAS No.: 40287-79-4
• Molecular Formula: C₁₅H₁₃N₃OSe
• Molecular Weight: 330.248
• Mol file: 40287-79-4.mol

Synonyms:2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole

Chemical Property of 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole

There total 4 articles about 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzaldehyd-<4-p-methoxy-phenyl-selenosemicarbazon> (14223-64-4) → 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole (40287-79-4)

Guidance literature:

With N-Bromosuccinimide; sodium acetate; In dichloromethane; for 2h; Reflux;

DOI:10.3184/174751916X14558161990884

Reference yield:

1-benzoyl-4-(4-methoxy-phenyl)-selenosemicarbazide (40287-61-4) → 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole (40287-79-4)

Guidance literature:

With acetyl chloride; In acetic acid; Heating;

Reference yield:

C8H11N3OSe → 2-(4-methoxyphenylamino)-5-phenyl-1,3,4-selenadiazole (40287-79-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / dichloromethane / 1 h / 20 °C

2: N-Bromosuccinimide; sodium acetate / dichloromethane / 2 h / Reflux

With N-Bromosuccinimide; sodium acetate; acetic acid; In dichloromethane;

DOI:10.3184/174751916X14558161990884

upstream raw materials:

1-benzoyl-4-(4-methoxy-phenyl)-selenosemicarbazide

Benzaldehyd-<4-p-methoxy-phenyl-selenosemicarbazon>

4-methoxyphenyl isoselenocyanate

Refernces