C₃₃H₄₀O₆

Base Information

Chemical Name:C₃₃H₄₀O₆
CAS No.:1264756-55-9
Molecular Formula:C₃₃H₄₀O₆
Molecular Weight:532.677
Hs Code.:

C<sub>33</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C₃₃H₄₀O₆

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Chemical Property of C₃₃H₄₀O₆

Chemical Property:

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Technology Process of C₃₃H₄₀O₆

There total 18 articles about C₃₃H₄₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₂O₆

: 1264756-55-9
C₃₃H₄₀O₆

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; Molecular sieve;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: C₄₄H₅₂O₅Si

: 1264756-55-9
C₃₃H₄₀O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: water; potassium hydroxide / tetrahydrofuran; methanol

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

2.2: 20 °C

3.1: diisobutylaluminium hydride / dichloromethane / -78 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

5.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

8.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

9.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

9.2: 20 °C

10.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

11.1: diethyl ether / -78 °C

12.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; tetrapropylammonium perruthennate; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 2.1: Swern oxidation / 2.2: Wittig reaction / 4.1: Sharpless asymmetric epoxidation / 6.1: Wittig reaction / 11.1: Grignard reaction;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-61-7
C₂₈H₃₄O₅

: 1264756-55-9
C₃₃H₄₀O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane / -78 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

4.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

7.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

8.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

8.2: 20 °C

9.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

10.1: diethyl ether / -78 °C

11.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; tetrapropylammonium perruthennate; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Swern oxidation / 1.2: Wittig reaction / 3.1: Sharpless asymmetric epoxidation / 5.1: Wittig reaction / 10.1: Grignard reaction;
DOI:10.1016/j.tetlet.2010.11.127