2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

Base Information

Chemical Name:2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride
CAS No.:1333500-49-4
Molecular Formula:C₁₆H₂₁Cl₂N₅*ClH
Molecular Weight:390.743
Hs Code.:

Synonyms:2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

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Chemical Property of 2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

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Technology Process of 2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

There total 3 articles about 2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.4%

: 743420-78-2
N-1-(2,3-dichloro)benzylbiguanide hydrochloride

: 502-42-1
cycloheptanone

: 1333500-49-4
2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

Guidance literature:: With hydrogenchloride; orthoformic acid triethyl ester; In methanol; water; at 20 ℃;
DOI:10.1016/j.bmcl.2011.06.125

Reference yield:

: 49552-34-3
(3,4-dichlorophenyl)methylammonium chloride

: 1333500-49-4
2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 160 - 180 °C

2: hydrogenchloride; orthoformic acid triethyl ester / methanol; water / 20 °C

With hydrogenchloride; orthoformic acid triethyl ester; In methanol; water;
DOI:10.1016/j.bmcl.2011.06.125

Reference yield:

: 102-49-8
3,4-dichlorobenzyl amine

: 1333500-49-4
2,4-diamino-5-(3',4'-dichlorobenzyl)-1,3,5-triazaspiro[5.6]dodeca-1,3-diene hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / diethyl ether / 20 °C

2: 160 - 180 °C

3: hydrogenchloride; orthoformic acid triethyl ester / methanol; water / 20 °C

With hydrogenchloride; orthoformic acid triethyl ester; In methanol; diethyl ether; water;
DOI:10.1016/j.bmcl.2011.06.125