N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

Base Information

Chemical Name:N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester
CAS No.:85472-92-0
Molecular Formula:C₄₅H₄₆N₄O₉
Molecular Weight:786.882
Hs Code.:

Synonyms:N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

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Chemical Property of N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

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Technology Process of N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

There total 6 articles about N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 21209-51-8
N-(Benzyloxycarbonyl)-L-serin-benzylester

: 110797-31-4
Ethyl-2-azido-3,4,6-tri-O-benzyl-2-desoxy-1-thio-β-D-galactopyranosid

: 110797-33-6
N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-galactopyranosyl)-L-serin-benzylester

: 85472-92-0
N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

Guidance literature:: With methyl trifluoromethanesulfonate; In diethyl ether; for 14h; Yields of byproduct given; Ambient temperature;

Reference yield:

: 68733-05-1
3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl nitrate

: 85472-92-0
N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / ethanol / 12 h / Ambient temperature

2: 67 percent / NaI / acetone / 14 h / Heating

3: 93 percent / 1percent NaOMe / methanol / 10 h / Ambient temperature

4: 1.) NaH / 1.) DMF, 0.5 h, 0 deg C, 2.) DMF, 3 h, r. t.

5: 68 percent / methyl triflate / diethyl ether / 14 h / Ambient temperature

With sodium methylate; sodium hydride; methyl trifluoromethanesulfonate; sodium iodide; In methanol; diethyl ether; ethanol; acetone;

Reference yield:

: 110797-26-7
3,4,6-Tri-O-acetyl-2-azido-2-desoxy-β-D-galactopyranosyl-ethylxanthogenat

: 85472-92-0
N-(Benzyloxycarbonyl)-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-galactopyranosyl)-L-serin-benzylester

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / NaI / acetone / 14 h / Heating

2: 93 percent / 1percent NaOMe / methanol / 10 h / Ambient temperature

3: 1.) NaH / 1.) DMF, 0.5 h, 0 deg C, 2.) DMF, 3 h, r. t.

4: 68 percent / methyl triflate / diethyl ether / 14 h / Ambient temperature

With sodium methylate; sodium hydride; methyl trifluoromethanesulfonate; sodium iodide; In methanol; diethyl ether; acetone;