dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH₂Cl₂

Base Information

• Chemical Name: dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH₂Cl₂
• CAS No.: 98677-57-7
• Molecular Formula: CH₂Cl₂*C₂₆H₂₆Cl₂P₂Pd
• Molecular Weight: 662.699

Synonyms:dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH₂Cl₂

Chemical Property of dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH₂Cl₂

Chemical Property:

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Technology Process of dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH₂Cl₂

There total 1 articles about dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(1-phenyl-3,4-dimethylphosphole)2PdCl2 (72937-30-5,66368-11-4,73244-96-9) + {Pd(II)Cl2(diphenylvinylphosphine)2} (78629-73-9,113214-83-8,98717-39-6) → dichloro{2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene}palladium(II)*CH2Cl2 (98677-57-7)

Guidance literature:

With CH₂Cl₂; In neat (no solvent); addn. of 1 equiv. of the vinylphosphine complex to 1 equiv. of the phosphole complex in solvent at ambient temp. under N2, react. time 24-48 h; according to the method described by Holt, M. S.; Nelson, J. H. et al. J. Am. Chem. Soc. 1985, 107, 6936; elem. anal.;

upstream raw materials:

(1-phenyl-3,4-dimethylphosphole)2PdCl₂

{Pd(II)Cl₂(diphenylvinylphosphine)2}

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