C₂₂H₂₄N₂O

Base Information

Chemical Name:C₂₂H₂₄N₂O
CAS No.:1416772-50-3
Molecular Formula:C₂₂H₂₄N₂O
Molecular Weight:332.445
Hs Code.:

C<sub>22</sub>H<sub>24</sub>N<sub>2</sub>O

Synonyms:C₂₂H₂₄N₂O

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Chemical Property of C₂₂H₂₄N₂O

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Technology Process of C₂₂H₂₄N₂O

There total 8 articles about C₂₂H₂₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1416772-49-0
C₂₃H₂₄N₂O₂

: 1416772-50-3
C₂₂H₂₄N₂O

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ml300385q

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 1416772-50-3
C₂₂H₂₄N₂O

Guidance literature:: Multi-step reaction with 6 steps

1: sodium acetate; acetic anhydride / 18 h / 115 °C / Inert atmosphere; Schlenk technique

2: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

3: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

4: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

5: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

6: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

With lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; sodium acetate; acetic anhydride; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether;
DOI:10.1021/ml300385q

Reference yield:

: 95200-94-5
(S)-N-acetyl-(pyridin-3-yl)alanine methyl ester

: 1416772-50-3
C₂₂H₂₄N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

2: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

3: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

With lithium aluminium tetrahydride; thionyl chloride; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether;
DOI:10.1021/ml300385q