2-(3-BROMOPHENOXY)PYRIDINE 97+%

Base Information

• Chemical Name: 2-(3-BROMOPHENOXY)PYRIDINE 97+%
• CAS No.: 92545-83-0
• Molecular Formula: C11H8BrNO
• Molecular Weight: 250.095
• Hs Code.: 2933399090
• Mol file: 92545-83-0.mol

Synonyms:Pyridine,2-(m-bromophenoxy)- (7CI);2-(3-Bromophenoxy)pyridine 97+%;2-(3-Bromophenoxy)pyridine;

Chemical Property of 2-(3-BROMOPHENOXY)PYRIDINE 97+%

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 63-64 °C
• Refractive Index: 1.607
• Boiling Point: 324.025 °C at 760 mmHg
• Flash Point: 149.765 °C
• PSA: 22.12000
• Density: 1.476 g/cm³
• LogP: 3.63640

Purity/Quality:

98%min ^*data from raw suppliers

2-(3-Bromophenoxy)pyridine 97.0% ^*data from reagent suppliers

Safty Information:

• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3-BROMOPHENOXY)PYRIDINE 97+%

There total 3 articles about 2-(3-BROMOPHENOXY)PYRIDINE 97+% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-bromo-pyridine (109-04-6) + 3-Bromophenol (591-20-8) → 2-(3-bromophenoxy)pyridine (92545-83-0)

Guidance literature:

With 2-Picolinic acid; potassium phosphate; copper(l) iodide; In dimethyl sulfoxide; at 90 ℃; for 24h; Inert atmosphere;

Reference yield: 62.0%

2-hydroxypyridin (142-08-5) + 1-Bromo-3-iodobenzene (591-18-4) → 2-(3-bromophenoxy)pyridine (92545-83-0)

Guidance literature:

With copper(l) iodide; potassium carbonate; L-proline; at 130 ℃; for 24h;

Reference yield:

→ 2-(3-bromophenoxy)pyridine (92545-83-0)

Guidance literature:

2-Brom-pyridin, 3-Bromphenol, wfr. K2CO3 bei 200-210grad;

DOI:10.1021/jo01067a058

upstream raw materials:

2-bromo-pyridine

3-Bromophenol

2-hydroxypyridin

1-Bromo-3-iodobenzene

Downstream raw materials:

(4-bromo-2-(pyridin-2-yloxy)phenyl)(phenyl)methanone

2-(3-(3-(1H-imidazol-1-yl)phenoxy)phenoxy)pyridine

3-methyl-1-(3-(3-(pyridin-2-yloxy)phenoxy)phenyl)-1H-imidazol-3-ium iodide

F₆P^(1-)*C₂₁H₁₈N₃O₂⁽¹⁺⁾

Refernces

• 1、 -. "ORGANOMETALLIC COMPOUND, ORGANIC LIGHT-EMITTING DEVICE INCLUDING THE ORGANOMETALLIC COMPOUND, AND DIAGNOSTIC COMPOSITION INCLUDING THE ORGANOMETALLIC COMPOUND". Paragraph 0250-0253. . Retrieved 2020/07/16.
• 2、 -. "ORGANOMETALLIC COMPOUND AND ORGANIC LIGHT-EMITTING DEVICE INCLUDING THE SAME". Paragraph 0384; 0386. . Retrieved 2020/06/16.