(3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Base Information

Chemical Name:(3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol
CAS No.:173537-09-2
Molecular Formula:C₃₇H₅₂O₈Si
Molecular Weight:652.901
Hs Code.:

Synonyms:(3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Suppliers and Price of (3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

There total 19 articles about (3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 173537-08-1
(3Z,10E,12E)-3-(methoxymethoxy)methyl-1-acetoxy-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-triene

: 173537-09-2
(3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Guidance literature:: With potassium carbonate; In methanol; for 3h; Ambient temperature;

Reference yield: 78.0%

: 2-[(3E,5E)-7-(tert-Butyl-diphenyl-silanyloxy)-hepta-3,5-dienyl]-2-[(Z)-6-(2,2-dimethyl-propionyloxy)-4-methoxymethoxymethyl-hex-3-enyl]-malonic acid dimethyl ester

: 173537-09-2
(3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Guidance literature:: With methanol; sodium methylate; Ambient temperature;
DOI:10.1016/S0040-4039(00)79137-4

Reference yield:

: 173536-84-0
(E,E)-8-tert-butyldiphenylsiloxy-1,1-bis(methoxycarbonyl)-4,6-octadiene

: 173537-09-2
(3Z,10E,12E)-3-(methoxymethoxy)methyl-7,7-bis(methoxycarbonyl)-14-tert-butyldiphenylsiloxytetradeca-3,10,12-trienol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH, 2.) KI / 1.) DMF, 40 deg C, 1 h, 2.) DMF, THF, 75 deg C, 12 h

2: 100 percent / K₂CO₃ / methanol / 3 h / Ambient temperature

With sodium hydride; potassium carbonate; potassium iodide; In methanol;