Technology Process of C26H32O5
There total 6 articles about C26H32O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lead(IV) acetate; sodium hydrogencarbonate;
In
dichloromethane;
for 0.833333h;
DOI:10.1021/ol9902374
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 10.8 g / TMSOTf; activated molecular sieves 4 Angstroem / CH2Cl2; tetrahydrofuran / 1 h / 0 °C
2: 5.0 g / TBAF; AcOH / tetrahydrofuran / 2 h / 20 °C
3: tetrahydrofuran; diethyl ether / 1 h / -78 - -20 °C
4: NaHCO3; Pb(OAc)4 / CH2Cl2 / 0.83 h
With
lead(IV) acetate; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol9902374
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; diethyl ether / 1 h / -78 - -20 °C
2: NaHCO3; Pb(OAc)4 / CH2Cl2 / 0.83 h
With
lead(IV) acetate; sodium hydrogencarbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol9902374