N,2-dihydroxy-5-methylbenzamide

Base Information

Chemical Name:N,2-dihydroxy-5-methylbenzamide
CAS No.:61799-77-7
Molecular Formula:C₈H₉NO₃
Molecular Weight:167.164
Hs Code.:2924299090
DSSTox Substance ID:DTXSID80381869
Wikidata:Q82173013
Mol file:61799-77-7.mol

Synonyms:N,2-dihydroxy-5-methylbenzamide;61799-77-7;2,N-dihydroxy-5-methyl-benzamide;SCHEMBL1759402;SCHEMBL12636131;5-methyl -salicylhydroxamic acid;DTXSID80381869;AQZRRKBZDRLEHU-UHFFFAOYSA-N;MFCD00176856;2-Hydroxy-5-methylbenzhydroxamic acid;AKOS000167392;CS-0262342;FT-0629335;EN300-82174;Z90126227

Suppliers and Price of N,2-dihydroxy-5-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N,2-dihydroxy-5-methylbenzamide
10mg
$ 45.00

American Custom Chemicals Corporation
N,2-DIHYDROXY-5-METHYLBENZAMIDE 95.00%
2.5G
$ 1499.48

American Custom Chemicals Corporation
N,2-DIHYDROXY-5-METHYLBENZAMIDE 95.00%
1G
$ 998.08

Advanced Chemicals Intermediatesced Chemicals Intermediates
2,N-Dihydroxy-5-methyl-benzamide 95%+
1g
$ 471.25

Acints
2,N-Dihydroxy-5-methyl-benzamide 95%+
1g
$ 471.25

Total 7 raw suppliers

Chemical Property of N,2-dihydroxy-5-methylbenzamide

Chemical Property:

PSA：69.56000
Density:1.332g/cm³
LogP:1.21050
XLogP3:2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:167.058243149
Heavy Atom Count:12
Complexity:172

Purity/Quality:

97% ^*data from raw suppliers

N,2-dihydroxy-5-methylbenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)O)C(=O)NO

Technology Process of N,2-dihydroxy-5-methylbenzamide

There total 1 articles about N,2-dihydroxy-5-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61799-77-7
2,N-dihydroxy-5-methylbenzamide

Guidance literature:

Reference yield:

: 61799-77-7
2,N-dihydroxy-5-methylbenzamide

: 1299489-77-2
5-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzo[d]isoxazol-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Reflux

1.2: pH 1

2.1: toluene-4-sulfonic acid; pyridine / tetrahydrofuran / 2 h / 75 °C / sealed tube

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 3.5 h

4.1: potassium carbonate / N,N-dimethyl-formamide

5.1: hydrogenchloride / water; methanol

With hydrogenchloride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; 1,1'-carbonyldiimidazole; pyridine; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; tetrachloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 61799-77-7
2,N-dihydroxy-5-methylbenzamide

: 1299489-85-2
[5-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzo[d]isoxazol-3-yloxy]-acetic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Reflux

1.2: pH 1

2.1: toluene-4-sulfonic acid; pyridine / tetrahydrofuran / 2 h / 75 °C / sealed tube

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 3.5 h

4.1: potassium carbonate / N,N-dimethyl-formamide

5.1: hydrogenchloride / water; methanol

6.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

7.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 2 h / 20 °C

With hydrogenchloride; N-Bromosuccinimide; lithium hydroxide monohydrate; 2,2'-azobis(isobutyronitrile); potassium carbonate; caesium carbonate; 1,1'-carbonyldiimidazole; pyridine; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; tetrachloromethane; water; N,N-dimethyl-formamide;