(syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

Base Information

Chemical Name:(syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol
CAS No.:140854-88-2
Molecular Formula:C₂₂H₃₈O₂Si
Molecular Weight:362.628
Hs Code.:

(syn)-3-<dimethyl(1,1,2-trimethylpropyl)silyl>-3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

Synonyms:(syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

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Technology Process of (syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

There total 7 articles about (syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 140854-57-5,140854-58-6
1-<oxy>-3-<2-(3-methylbutenyl)oxy>-1-phenyl-3-(phenylthio)propane

: 140854-88-2
(syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

: 140854-89-3
(anti)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

Guidance literature:: With lithium 1-naphthalenide; In tetrahydrofuran; at -78 ℃; for 0.5h;

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 140854-88-2
(syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) KH / 1) THF, 30 min, 2) THF, r.t.

2: 1) O₃, 2) PPh₃ / 1) CH₂Cl₂, -78 deg C, 2) CH₂Cl₂, r.t.

3: 1) Me₃SiOSO₂CF₃ / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂

4: 26 percent / Li-naphth / tetrahydrofuran / 0.5 h / -78 °C

With trimethylsilyl trifluoromethanesulfonate; potassium hydride; lithium 1-naphthalenide; ozone; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 71821-61-9
3-methyl-1-(trimethylsilyloxy)but-2-ene

: 140854-88-2
(syn)-3--3-<(3-methyl)-2-butenyloxy>-1-phenylpropanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Me₃SiOSO₂CF₃ / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂

2: 26 percent / Li-naphth / tetrahydrofuran / 0.5 h / -78 °C

With trimethylsilyl trifluoromethanesulfonate; lithium 1-naphthalenide; In tetrahydrofuran;