10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane

Base Information

• Chemical Name: 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane
• CAS No.: 209733-24-4
• Molecular Formula: C₁₉H₂₉BOSi
• Molecular Weight: 312.335
• Mol file: 209733-24-4.mol

Synonyms:10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane

Chemical Property of 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane

There total 1 articles about 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

9-borabicyclo{3.3.1}nonane + 1-Phenyl-2-(trimethylsilyl)acetylene (2170-06-1) → 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane (209733-24-4)

Guidance literature:

DOI:10.1016/S0040-4039(98)00750-3

Reference yield: 97.0%

2-bromo-pyridine (109-04-6) + 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane (209733-24-4) → 2-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-pyridine

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 5h;

DOI:10.1016/S0040-4039(98)00750-3

Reference yield: 59.0%

bromobenzene (108-86-1,52753-63-6) + 10-((Z)-2-Phenyl-1-trimethylsilanyl-vinyl)-9-oxa-10-bora-bicyclo[3.3.2]decane (209733-24-4) → (Z)-(1,2-diphenylvinyl)-trimethylsilane (57266-94-1)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 6h;

DOI:10.1016/S0040-4039(98)00750-3

upstream raw materials:

1-Phenyl-2-(trimethylsilyl)acetylene

Downstream raw materials:

(Z)-(1,2-diphenylvinyl)-trimethylsilane