8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

Base Information

Chemical Name:8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate
CAS No.:67171-61-3
Molecular Formula:C₁₇H₁₄ClN₄*HO₄S
Molecular Weight:406.849
Hs Code.:

Synonyms:8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

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Chemical Property of 8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

Chemical Property:

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Technology Process of 8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

There total 4 articles about 8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-51-0
orthoformic acid triethyl ester

: 56167-78-3
7-chloro-2-(N-methyl-hydrazino)-5-phenyl-3H-benzo[e][1,4]diazepine

: 67171-61-3
8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

Guidance literature:: With sulfuric acid; In chloroform;

Reference yield:

: 122-51-0
orthoformic acid triethyl ester

: 56167-78-3
7-chloro-2-(N-methyl-hydrazino)-5-phenyl-3H-benzo[e][1,4]diazepine

: 67171-61-3
8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

: 56167-84-1
8-Chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium chloride

Guidance literature:: With sulfuric acid; In chloroform;

Reference yield:

: 4547-02-8
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione

: 67171-61-3
8-chloro-3-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepinium hydrogen sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: sulfuric acid / chloroform

With sulfuric acid; In methanol; chloroform;