methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

Base Information

Chemical Name:methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate
CAS No.:931415-42-8
Molecular Formula:C₂₇H₃₆N₂O₁₂
Molecular Weight:580.589
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

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Chemical Property of methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

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Technology Process of methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

There total 5 articles about methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 869996-05-4
O-(methyl 2,3,4-tri-O-acetyl-D-glucuronopyranosyl)-N-phenyl-2,2,2-trifluoroacetimidate

: 149647-78-9
vorinostat

: 931415-42-8
methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃;
DOI:10.1021/jo0701839

Reference yield: 73.0%

: 149648-52-2
suberanilic acid

: 319926-20-0
(2S,3S,4S,5R,6S)-3,4,5-Triacetoxy-6-aminooxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 931415-42-8
methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2006.11.042

Reference yield:

: 72692-06-9,73464-50-3,3082-95-9
methyl 2,3,4-tri-O-acetyl-D-glucopyranuronate

: 931415-42-8
methyl 2,3,4-tri-O-acetyl-1-O-7-(phenylcarbamoyl)hepthydroxamoyl-β-D-glucopyranosyluronate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / CH₂Cl₂ / 20 °C

2: 76 percent / TMSOTf / CH₂Cl₂ / -20 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; potassium carbonate; In dichloromethane;
DOI:10.1021/jo0701839