Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Base Information

Chemical Name:Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester
CAS No.:399551-06-5
Molecular Formula:C₂₂H₃₂O₃
Molecular Weight:344.494
Hs Code.:

Synonyms:Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Suppliers and Price of Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

There total 3 articles about Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2Z,4E,8E)-(6S,7S)-6-hydroxy-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

: 399551-06-5
Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/jo010648+

Reference yield:

: 399550-96-0
13-cis-11,12-didehydro-9,10-dihydro-10-hydroxyretinol

: 399551-06-5
Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 16 h / 20 °C

2: 89.5 percent / 2,4,6-collidine / 48 h / 20 °C

3: PCC / CH₂Cl₂ / 3 h / 0 °C

With 2,4,6-trimethyl-pyridine; lithium aluminium tetrahydride; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1021/jo010648+

Reference yield:

: (9R*,10S*)-13-cis-9,10-dihydro-10-hydroxyretinol

: 399551-06-5
Acetic acid (2Z,4E,8E)-3,7-dimethyl-6-oxo-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,8-trienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89.5 percent / 2,4,6-collidine / 48 h / 20 °C

2: PCC / CH₂Cl₂ / 3 h / 0 °C

With 2,4,6-trimethyl-pyridine; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jo010648+