Technology Process of C32H23BrClF3N6
There total 10 articles about C32H23BrClF3N6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C32H24ClF3N6;
With
bromine; acetic acid;
at 20 ℃;
With
sodium sulfite;
In
water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 0.33 h / Cooling with ice
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.67 h / -78 - 20 °C
3: hydrazine / 1,4-dioxane / 1 h / 20 °C
4: boron trifluoride diethyl etherate / methanol / 1.5 h / 100 °C / sealed tube
5: ethylenediamine; copper(l) iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C
6: 0.75 h / 140 °C
7: bromine; acetic acid / 20 °C
With
copper(l) iodide; boron trifluoride diethyl etherate; bromine; acetic acid; ethylenediamine; 3-chloro-benzenecarboperoxoic acid; hydrazine;
In
1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 - 0 °C
1.2: 1 h / 20 °C
2.1: boron trifluoride diethyl etherate / methanol / 1.5 h / 100 °C / sealed tube
3.1: ethylenediamine; copper(l) iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C
4.1: 0.75 h / 140 °C
5.1: bromine; acetic acid / 20 °C
With
copper(l) iodide; boron trifluoride diethyl etherate; bromine; sodium hexamethyldisilazane; acetic acid; ethylenediamine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
