(E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

Base Information

Chemical Name:(E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one
CAS No.:1352061-35-8
Molecular Formula:C₂₁H₃₀O₅
Molecular Weight:362.466
Hs Code.:

Synonyms:(E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

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Chemical Property of (E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

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Technology Process of (E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

There total 6 articles about (E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₃₅H₄₂O₅

: 1352061-35-8
(E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

Guidance literature:: C₃₅H₄₂O₅; With sodium methylate; In methanol; at 0 ℃; for 12h;

In methanol;

Reference yield: 88.0%

: C₃₅H₃₈O₇

: 1352061-35-8
(E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

Guidance literature:: With sodium methylate; In methanol; at 0 ℃; for 8h;
DOI:10.2174/1573406411666150514100630

Reference yield:

: 129234-94-2
(S)-2-hydroxy-7-octene

: 1352061-35-8
(E)-1-[(5R)-5-(3,6-dideoxy-α-L-arabino-hexopyranosyloxy)hexyl]-3-phenyl-2-propen-1-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

1.2: 3 h / -20 °C

2.1: palladium dichloride; copper(l) chloride; oxygen / N,N-dimethyl-formamide; water / 4 h / 20 °C

3.1: pyrrolidine / dichloromethane / 18 h / 20 °C

4.1: sodium methylate / methanol / 8 h / 0 °C

With pyrrolidine; oxygen; sodium methylate; copper(l) chloride; palladium dichloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; 3.1: |Aldol Condensation;
DOI:10.2174/1573406411666150514100630