(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

Base Information

Chemical Name:(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate
CAS No.:1431563-79-9
Molecular Formula:C₂₄H₃₄O₅Si
Molecular Weight:430.616
Hs Code.:

Synonyms:(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

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Technology Process of (2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

There total 1 articles about (2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 153974-48-2
3-methoxy-O-tert-butyldimethylsilylbenzyl alcohol

: 384365-49-5
methyl 2-diazo-2-(3-methoxyphenyl)acetate

: 1431563-79-9
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

Guidance literature:: With dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leucinate]; at 50 ℃; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja401731d

Reference yield: 87.0%

: 1431563-79-9
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

: 1431563-93-7
(2S,3S)-methyl 3-hydroxy-2-(3-methoxyphenyl)-3-(4-methoxyphenyl)propanoate

Guidance literature:: With hydrogenchloride; In ethanol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja401731d

Reference yield:

: 1431563-79-9
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-bis(3-methoxyphenyl)propanoate

: 1431564-04-3
(2S,3S)-methyl 5-methoxy-2-(3-methoxyphenyl)-2,3-dihydrobenzofuran-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / 0 - 20 °C / Inert atmosphere

2: [bis(acetoxy)iodo]benzene; lithium carbonate; palladium diacetate / Hexafluorobenzene / 24 h / 100 °C / Inert atmosphere

With hydrogenchloride; [bis(acetoxy)iodo]benzene; palladium diacetate; lithium carbonate; In Hexafluorobenzene; ethanol;
DOI:10.1021/ja401731d