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moenocinol benzyl ether

Base Information
  • Chemical Name:moenocinol benzyl ether
  • CAS No.:87957-22-0
  • Molecular Formula:C32H48O
  • Molecular Weight:448.733
  • Hs Code.:
moenocinol benzyl ether

Synonyms:moenocinol benzyl ether

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Chemical Property of moenocinol benzyl ether
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Technology Process of moenocinol benzyl ether

There total 19 articles about moenocinol benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 85 percent / 1.5M-n-BuLi / hexane; tetrahydrofuran
2: 1.) lithium di-isopropylamide, 2.) hexamethylphosphoric triamide, 3.) n-Bu4NF*3H2O
With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; tetrabutyl ammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1039/P19830001777
Guidance literature:
Multi-step reaction with 8 steps
1: 3.10 g / KOH / methanol / 1 h / Heating
2: 90 percent / 1.43M-n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 20 min, 2.) room temperature, 2.5 h
3: 85 percent / 5.65percent Na(Hg) / tetrahydrofuran; methanol / 135.84 h / 20 °C
4: 100 percent / Et3N / CH2Cl2 / 1 h / 0 °C
5: 98 percent / NaI / acetone / 16 h / Heating
6: 83 percent / 1.5M-n-BuLi / tetrahydrofuran / 3 h / Ambient temperature
7: 85 percent / 1.5M-n-BuLi / hexane; tetrahydrofuran
8: 1.) lithium di-isopropylamide, 2.) hexamethylphosphoric triamide, 3.) n-Bu4NF*3H2O
With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; n-butyllithium; sodium amalgam; tetrabutyl ammonium fluoride; triethylamine; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; acetone;
DOI:10.1039/P19830001777
Guidance literature:
Multi-step reaction with 7 steps
1: 90 percent / 1.43M-n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 20 min, 2.) room temperature, 2.5 h
2: 85 percent / 5.65percent Na(Hg) / tetrahydrofuran; methanol / 135.84 h / 20 °C
3: 100 percent / Et3N / CH2Cl2 / 1 h / 0 °C
4: 98 percent / NaI / acetone / 16 h / Heating
5: 83 percent / 1.5M-n-BuLi / tetrahydrofuran / 3 h / Ambient temperature
6: 85 percent / 1.5M-n-BuLi / hexane; tetrahydrofuran
7: 1.) lithium di-isopropylamide, 2.) hexamethylphosphoric triamide, 3.) n-Bu4NF*3H2O
With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium amalgam; tetrabutyl ammonium fluoride; triethylamine; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; acetone;
DOI:10.1039/P19830001777
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