C₅₁H₈₂O₇Si₂

Base Information

Chemical Name:C₅₁H₈₂O₇Si₂
CAS No.:1361130-31-5
Molecular Formula:C₅₁H₈₂O₇Si₂
Molecular Weight:863.379
Hs Code.:

C<sub>51</sub>H<sub>82</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₅₁H₈₂O₇Si₂

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Chemical Property of C₅₁H₈₂O₇Si₂

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Technology Process of C₅₁H₈₂O₇Si₂

There total 20 articles about C₅₁H₈₂O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: C₅₁H₈₀O₇Si₂

: 1361130-31-5
C₅₁H₈₂O₇Si₂

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 35 ℃; for 3h;
DOI:10.1021/ol300182r

Reference yield:

: 1313835-58-3
(5R)-2,2,3,3,9,9,10,10-octamethyl-5-(prop-2-en-1-yl)-4,8-dioxa-3,9-disilaundecane

: 1361130-31-5
C₅₁H₈₂O₇Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 12 h / 20 °C

2.1: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C

3.1: titanium tetrachloride; sparteine / dichloromethane / 0 °C

3.2: 1 h / 0 °C

4.1: 2,6-di-tert-butyl-pyridine / dichloromethane / 18 h / 20 °C

5.1: lithium borohydride / tetrahydrofuran; methanol / 2.5 h / 0 - 20 °C

6.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

7.1: chromium dichloride / tetrahydrofuran / 3 h / 20 °C

8.1: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S / acetonitrile / 3 h / 20 °C

9.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 35 °C

With chromium dichloride; sodium periodate; osmium(VIII) oxide; lithium borohydride; 2,6-di-tert-butyl-pyridine; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S; palladium 10% on activated carbon; water; hydrogen; titanium tetrachloride; Dess-Martin periodane; 4-methylmorpholine N-oxide; sparteine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile; 3.1: Evans asymmetric aldol reaction / 3.2: Evans asymmetric aldol reaction / 6.1: Dess-Martin oxidation / 7.1: Takai olefination / 8.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1021/ol300182r

Reference yield:

: 1361130-12-2
C₃₁H₅₅NO₆Si₂

: 1361130-31-5
C₅₁H₈₂O₇Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: lithium borohydride / tetrahydrofuran; methanol / 2.5 h / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

3: chromium dichloride / tetrahydrofuran / 3 h / 20 °C

4: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S / acetonitrile / 3 h / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 35 °C

With chromium dichloride; lithium borohydride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S; palladium 10% on activated carbon; hydrogen; Dess-Martin periodane; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile; 2: Dess-Martin oxidation / 3: Takai olefination / 4: Nozaki-Hiyama-Kishi reaction;
DOI:10.1021/ol300182r