<<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine

Base Information

• Chemical Name: <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine
• CAS No.: 122225-50-7
• Molecular Formula: C₁₆H₂₄N₂O₆
• Molecular Weight: 340.376
• Mol file: 122225-50-7.mol

Synonyms:<<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine

Chemical Property of <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine

There total 5 articles about <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

<<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine methyl ester (122225-49-4) → <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine (122225-50-7)

Guidance literature:

With lithium hydroxide; In 1,4-dioxane; at 0 ℃; for 1h;

DOI:10.1021/jm00169a024

Reference yield:

2-<<(benzyloxy)carbonyl>methylamino>-1-(methoxymethoxy)ethane (122225-41-6) → <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine (122225-50-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 84 percent / H₂ / 10percent Pd/C / methanol / 12 h

2: 58 percent / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, overnight

3: 100 percent / aq. LiOH / dioxane / 1 h / 0 °C

With lithium hydroxide; hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane;

DOI:10.1021/jm00169a024

Reference yield:

1-(methoxymethoxy)-2-(methylamino)ethane (122225-44-9) → <<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine (122225-50-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 58 percent / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, overnight

2: 100 percent / aq. LiOH / dioxane / 1 h / 0 °C

With lithium hydroxide; In 1,4-dioxane; dichloromethane;

DOI:10.1021/jm00169a024

upstream raw materials:

<<<2-(methoxymethoxy)ethyl>methylamino>carbonyl>-O-methyltyrosine methyl ester

1-(methoxymethoxy)-2-(methylamino)ethane

2-<<(benzyloxy)carbonyl>methylamino>-1-(methoxymethoxy)ethane

α-isocyanato-L-O-methyltyrosine methyl ester