2,4,6-tris(bromomethyl)-N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

Base Information

• Chemical Name: 2,4,6-tris(bromomethyl)-N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine
• CAS No.: 1377871-01-6
• Molecular Formula: C₃₉H₆₀Br₃N₃O₁₂
• Molecular Weight: 1002.63

Synonyms:2,4,6-tris(bromomethyl)-N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

Chemical Property of 2,4,6-tris(bromomethyl)-N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of 2,4,6-tris(bromomethyl)-N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

There total 5 articles about 2,4,6-tris(bromomethyl)-N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.9%

N1,N1,N3,N3,N5,N5-hexakis(tertbutoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine (1377871-00-5) → 2,4,6-tris(bromomethyl)-N1,N1,N3,N3,N5,N5-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine (1377871-01-6)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 5h; Irradiation;

DOI:10.1080/10610278.2011.632822

Reference yield:

N1,N3,N5-tris(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine (1377870-97-7) → 2,4,6-tris(bromomethyl)-N1,N1,N3,N3,N5,N5-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine (1377871-01-6)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap / tetrahydrofuran / Reflux

2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / Irradiation

With dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tetrachloromethane;

DOI:10.1080/10610278.2011.632822

Reference yield:

2,4,6-trinitromesitylene (602-96-0) → 2,4,6-tris(bromomethyl)-N1,N1,N3,N3,N5,N5-hexakis(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine (1377871-01-6)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogenchloride; tin(ll) chloride / water / 5 h / 105 °C

2: tetrahydrofuran / 48 h / Reflux

3: dmap / tetrahydrofuran / Reflux

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / Irradiation

With hydrogenchloride; dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tin(ll) chloride; In tetrahydrofuran; tetrachloromethane; water;

DOI:10.1080/10610278.2011.632822

upstream raw materials:

N₁,N₃,N₅-tris(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

N₁,N₁,N₃,N₃,N₅,N₅-hexakis(tertbutoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

2,4,6-trinitromesitylene

1,3,5-trisamine-2,4,6-trimethylbenzene

Downstream raw materials:

2,4,6-tris(bromomethyl)-N₁,N₃,N₅-tris(tert-butoxycarbonyl)-2,4,6-trimethylbenzene-1,3,5-triamine

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