2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

Base Information

Chemical Name:2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester
CAS No.:73436-05-2
Molecular Formula:C₂₆H₃₂O₄
Molecular Weight:408.538
Hs Code.:

Synonyms:2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

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Chemical Property of 2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

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Technology Process of 2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

There total 6 articles about 2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106-24-1
Geraniol

: 16929-92-3
2,4-dihydroxy-6-phenethylbenzoic acid methyl ester

: 73436-05-2
2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

Guidance literature:: With boron trifluoride diethyl etherate; In 1,4-dioxane; at 20 ℃; for 48h;
DOI:10.1055/s-1991-26390

Reference yield:

: 2524-37-0
ethyl orselinate

: 73436-05-2
2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / pyridine / 4 h / Heating

2: 76 percent / Br₂ / CCl₄ / 1 h / 20 °C / Irradiation

3: 80 percent / toluene / 3 h / Heating

4: 1) NaOMe / 1) 30 min, 20 deg C 2) MeOH, 12 h, reflux

5: 96 percent / H₂ / 5percent Pd/C / methanol / 5 h / 20 °C / 3750.3 Torr

6: 62 percent / BF₃*Et₂O / dioxane / 48 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; hydrogen; bromine; sodium methylate; palladium on activated charcoal; In 1,4-dioxane; methanol; tetrachloromethane; toluene;
DOI:10.1055/s-1991-26390

Reference yield:

: 28520-50-5
2,4-Diacetoxy-6-methylbenzoesaeureethylester

: 73436-05-2
2,4-Dihydroxy-3-geranyl-6-phenethylbenzoesaeuremethylester

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / Br₂ / CCl₄ / 1 h / 20 °C / Irradiation

2: 80 percent / toluene / 3 h / Heating

3: 1) NaOMe / 1) 30 min, 20 deg C 2) MeOH, 12 h, reflux

4: 96 percent / H₂ / 5percent Pd/C / methanol / 5 h / 20 °C / 3750.3 Torr

5: 62 percent / BF₃*Et₂O / dioxane / 48 h / 20 °C

With boron trifluoride diethyl etherate; hydrogen; bromine; sodium methylate; palladium on activated charcoal; In 1,4-dioxane; methanol; tetrachloromethane; toluene;
DOI:10.1055/s-1991-26390